Hydrochloric Acid → HCID 136983871, compound

HRID 1507484Notes

Reaction equation

HRID 1507484 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[C:10]1[C:11](=[O:31])[NH:12][C:13]([S:29][CH3:30])=[N:14][C:15]=1[NH:16][C@H:17]1[C@H:24]2[C@H:20]([O:21]C(C)(C)[O:23]2)[C@@H:19]([CH2:27][OH:28])[CH2:18]1.Cl>CO>[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[C:10]1[C:11](=[O:31])[NH:12][C:13]([S:29][CH3:30])=[N:14][C:15]=1[NH:16][C@@H:17]1[CH2:18][C@H:19]([CH2:27][OH:28])[C@@H:20]([OH:21])[C@H:24]1[OH:23]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 136983947HCID 136983947, compound

Product 1

HCID 136983871HCID 136983871, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Compound 13 (15 mg, 0.033 mmol) was dissolved in MeOH (1 ml) and 3 M HCl (1 ml) and stirred at room temperature for 18 h. The solvents were evaporated to give the title compound as a white solid.

Workup

  1. customThe solvents were evaporated

Sources & evidence

ORD record
ord-ad0ae3e9bf87423596f3e9b5fafb74c0
Source dataset
uspto-grants-2015_12
Patent number
US09221809B2

Reaction notes

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