Hydrochloric Acid → HCID 136504460, compound

HRID 1507486Notes

Reaction equation

HRID 1507486 reaction equation
[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[C:10]1[C:11]([NH:20][C@H:21]2[C@@H:25]3[O:26]C(C)(C)[O:28][C@@H:24]3[C@@H:23]([CH2:31][OH:32])[CH2:22]2)=[N:12][C:13]([CH2:18][CH3:19])=[N:14][C:15]=1[O:16]C.Cl>CO>[S:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[CH:9][C:4]=2[N:3]=[C:2]1[C:10]1[C:15](=[O:16])[NH:14][C:13]([CH2:18][CH3:19])=[N:12][C:11]=1[NH:20][C@@H:21]1[CH2:22][C@H:23]([CH2:31][OH:32])[C@@H:24]([OH:28])[C@H:25]1[OH:26]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 117677809HCID 117677809, compound

Product 1

HCID 136504460HCID 136504460, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Compound 14 (48 mg, 0.108 mmol) was suspended in MeOH (3 ml) and 3 M HCl (3) was added. The mixture was stirred at room temperature for 18 h. The mixture was evaporated to dryness to give the title compound as a white solid.

Workup

  1. customThe mixture was evaporated to dryness

Sources & evidence

ORD record
ord-edc684b586b8486c8ac422d3ba834578
Source dataset
uspto-grants-2015_12
Patent number
US09221809B2

Reaction notes

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