HuagongsheHuagongshe Chemistry Print Report · For research reference only
7-Chloro-2-mercaptobenzothiazole → 7-Chloro-1,3-benzothiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 7-Chloro-2-mercaptobenzothiazole | HCID 178527784 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 7-Chloro-1,3-benzothiazole | HCID 18411293 | — |
Reaction Steps
Following the same procedure in step 2 of Example 337 using 7-chloro-1,3-benzothiazole-2-thiol (700 mg, 3.47 mmol, 1.00 equiv) and iron powder (1.94 g, 10.00 equiv) in acetic acid (20.0 mL) (gray white solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221809B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-0ff600dd649f4fccbf17228fe6539ee7 |
| Source note | uspto-grants-2015_12 |