HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178424007, compound → 7-Methylbenzo[d]thiazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178424007 | HCID 178424007 | — |
| Catalyst | Iron | HCID 23925 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | 7-Methylbenzo[d]thiazole | HCID 15655022 | — |
Reaction Steps
Following the same procedure as in step 2 of Example 337 using 7-methyl-1,3-benzothiazole-2-thiol (3.8 g, 20.96 mmol, 1.00 equiv) and iron powder (9.28 g, 171.85 mmol, 8.20 equiv) in acetic acid (24 mL) as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221809B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-44996eb4b7b4470eaa42aa80d52ddc8c |
| Source note | uspto-grants-2015_12 |