N-(4-fluorophenyl)-N-nitrosoglycine → HCID 178516722, compound

Participants

Role	Name	HCID	Charge
Reactant	N-(4-fluorophenyl)-N-nitrosoglycine	HCID 86729695	—
Solvent	Acetic Anhydride	HCID 7918	—
Product	HCID 178516722	HCID 178516722	106.6%

Reaction Conditions

Temperature	70 °C

Reaction Steps

N-(4-fluorophenyl)-N-nitrosoglycine (11.5 g, 54.7 mmol) was dissolved in acetic anhydride (100 mL) and heated to 70° C. for 14 h. The reaction mixture was cooled and then poured into ice water (300 mL) After for stirring for 30 m, the reaction mixture was filtered to provide 10.50 g (100%) of the title product.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US09221805B2
Source dataset	uspto-grants-2015_12
ORD ID	ord-b771a1d493a8425d875acc9a89b2f228
Source note	uspto-grants-2015_12