HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 56942175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 66758218 | HCID 66758218 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 56942175 | HCID 56942175 | — |
Reaction Steps
To a solution of the compound of example 338 (66 mg, 0.15 mmol) in dichloromethane (6 ml) was added trifluoroacetic acid (3 ml). The solution was stirred at room temperature for 30 minutes. The solvents were evaporated in vacuo and co-evaporated with toluene. The residue was directly used for further reaction without any purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221822B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-145cce083d80427b999d8ca4ac790a8c |
| Source note | uspto-grants-2015_12 |