Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1508182Generated: November 1, 2026

Pyrrolidine → HCID 71239270, compound

https://huagongshe.com/reaction/1508182

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyrrolidineHCID 31268—
ReactantHCID 15734662HCID 15734662—
SolventDichloromethaneHCID 6344—
SolventTetrahydrofuranHCID 8028—
ProductHCID 71239270HCID 71239270—

Reaction Conditions

Temperature0 °C

Reaction Steps

To a solution of 2-(2,4-dichlorophenyl)acrylic acid methyl ester (0.70 mmol) in 2 mL THF was added pyrrolidine (0.77 mmol) at 0° C. The reaction mixture was stirred at 0° C. for 50 min, diluted with DCM and washed with water. The organic layer was dried over MgSO4 and concentrated in vacuo to give the desired compound as pinkish oil;

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09221832B2
Source datasetuspto-grants-2015_12
ORD IDord-b45d0e0397444c31a5c1299951861095
Source noteuspto-grants-2015_12