HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 71239163, compound → HCID 86721945, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 71239163 | HCID 71239163 | — |
| Reactant | furo[2,3-c]pyridazin-5(6H)-one O-methyl oxime | HCID 86721901 | — |
| Product | HCID 86721945 | HCID 86721945 | — |
Reaction Steps
This compound was prepared using a method analogous to that of furo[2,3-c]pyridazin-5(6H)-one O-methyl oxime (A.2.3.3), 4-(trifluoromethyl)furo[2,3-b]pyridin-3(2H)-one replacing furo[2,3-c]pyridazin-5(6H)-one. Purification by (KP-SIL™ from Biotage) using Hept/EtOAc (9/1) gives the desired product as colorless foam;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221832B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-4ec45f39a5b74ea5b08b46d72838bcea |
| Source note | uspto-grants-2015_12 |