HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanamide → HCID 178512257, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanamide | HCID 9864 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | 5-Chloro-2-thiophenecarbonitrile | HCID 12203265 | — |
| Reactant | HCID 178418582 | HCID 178418582 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178512257 | HCID 178512257 | — |
Reaction Steps
To a solution of 5-chlorothiophene-2-carbonitrile 1 in MeOH was added NaOCH3. The reaction mixture was stirred at room temperature for 4 h and then NH2CN was added. The reaction was allowed stir for overnight under N2. The mixture was then poured into NH4Cl (aq) and the precipitate collected and washed with water. The dried sample was confirmed as desired product 5-chloro-N-cyanothiophene-2-carboximidamide 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221843B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-2b2e2c1a069d4abc9fd26b833e6bcf8c |
| Source note | uspto-grants-2015_12 |