HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1508701Generated: October 30, 2026
Nitrogen → 2-Chloro-4-(5-chloro-2-thienyl)-6-methyl-1,3,5-triazine
https://huagongshe.com/reaction/1508701
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178512257 | HCID 178512257 | — |
| Product | 2-Chloro-4-(5-chloro-2-thienyl)-6-methyl-1,3,5-triazine | HCID 74221040 | — |
Reaction Steps
To a solution of reactant 3 in CH3CN was added reactant 2 and POCl3. The mixture was stirred at 70° C. overnight under. N2. TLC showed starting material was consumed. The mixture was then poured into NaHCO3 (aq) carefully and the precipitate collected. The dried sample was confirmed as desired product 2-chloro-4-(5-chlorothiophen-2-yl)-6-methyl-1,3,5-triazine 4.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09221843B2 |
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| Source dataset | uspto-grants-2015_12 |
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| ORD ID | ord-3346b58509d749b7a4c3b4f6baa525ec |
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| Source note | uspto-grants-2015_12 |
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