HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 90338578, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 90338681 | HCID 90338681 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90338578 | HCID 90338578 | — |
Reaction Steps
Following general procedure C, tert-butyl 4-(4-((4-(2-ethoxy-2-oxoethyl)phenyl)amino)-6,7-dihydro-5H-cyclopenta[b]pyridin-2-yl)piperazine-1-carboxylate (0.034 g, 0.071 mmol) was reacted with ammonia in methanol (7.0 M, 5 mL) to afford crude product (0.031 g) as an orange oil. MW=451.56. APCI MS m/z 452 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221843B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-b36655e995b04a4c8a34c2b51d305ea5 |
| Source note | uspto-grants-2015_12 |