HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Diaminotoluene → HCID 59590552, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Diaminotoluene | HCID 10332 | — |
| Reactant | 4-Cyanobenzoic acid | HCID 12087 | — |
| Product | HCID 59590552 | HCID 59590552 | 68% |
Reaction Steps
The title compound (173 mg, 68% yield) was prepared as a grey solid from 4-cyano-benzoic acid (294 mg, 2 mmol) and 4-methyl-o-phenylenediamine (293 mg, 2.4 mmol) by an analogous procedure to that described in example 8. LC-MS (m/z) 256 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211901B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-bb2ae5682d2f4dda99ffe532ebf58a96 |
| Source note | uspto-grants-2012_07 |