HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanobenzoic acid → HCID 59590550, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanobenzoic acid | HCID 12087 | — |
| Reactant | 4-Methoxy-o-phenylenediamine | HCID 153404 | — |
| Product | HCID 59590550 | HCID 59590550 | 71% |
Reaction Steps
The title compound (192 mg, 71% yield) was prepared as a grey solid from 4-cyano-benzoic acid (294 mg, 2 mmol) and 4-methoxy-o-phenylenediamine (331 mg, 2.4 mmol) by an analogous procedure to that described in example 8. LC-MS (m/z) 272 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211901B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-338907a25b2f4502b23d4992fd83b3f7 |
| Source note | uspto-grants-2012_07 |