HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → HCID 59590547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 6-Cyanopyridine-3-carboxylic acid | HCID 2761108 | — |
| Product | HCID 59590547 | HCID 59590547 | 65% |
Reaction Steps
The title compound (157 mg, 65% yield) was prepared as a grey solid from 6-cyano-nicotinic acid (296 mg, 2 mmol) and o-phenylenediamine (864 mg, 8 mmol) by an analogous procedure to that described in example 8. LC-MS (m/z) 243 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211901B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-145fcb2328d546d28011e7cef47d068e |
| Source note | uspto-grants-2012_07 |