HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzene-1,2-diamine → HCID 59590554, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzene-1,2-diamine | HCID 164584 | — |
| Reactant | 6-Cyanopyridine-3-carboxylic acid | HCID 2761108 | — |
| Product | HCID 59590554 | HCID 59590554 | 52% |
Reaction Steps
The title compound (135 mg, 52% yield) was prepared as a grey solid from 6-cyano-nicotinic acid (296 mg, 2 mmol) and 4-fluoro-o-phenylenediamine (302 mg, 2.4 mmol) by an analogous procedure to that described in example 8. LC-MS (m/z) 261 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211901B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-a99dc2df0496466f9af333d56fc52faf |
| Source note | uspto-grants-2012_07 |