Hydrochloric Acid → HCID 68501486, compound

HRID 1510027Notes

Reaction equation

[CH3:1][C@@:2]12[CH2:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[C@@H:3]1[NH:4][CH2:5][CH2:6][CH2:7]2.[ClH:15]>>[ClH:15].[CH3:1][C@@:2]12[CH2:14][C:13]3[C:8](=[CH:9][CH:10]=[CH:11][CH:12]=3)[C@@H:3]1[NH:4][CH2:5][CH2:6][CH2:7]2

Participants

Reactant 2

HCID 313Hydrochloric Acid

HCID 42633844HCID 42633844, compound

Product 1

HCID 68501486HCID 68501486, compound

Procedure

(−)-(4aR,9bR)-4a-Methyl-2,3,4,4a,5,9b-hexahydro-1H-indeno[1,2-b]pyridine was made into a hydrochloride by a conventional method, and then recrystallized from ethyl acetate/ethanol to obtain (4aR,9bR)-4a-methyl-2,3,4,4a,5,9b-hexahydro-1H-indeno[1,2-b]pyridine hydrochloride as a colorless crystal.

Workup

customrecrystallized from ethyl acetate/ethanol

Sources & evidence

ORD record: ord-523c98ee32624a26a7c99162aca5e20a
Source dataset: uspto-grants-2012_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08211907B2

Reaction notes

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