HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 44160196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 66920434 | HCID 66920434 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 44160196 | HCID 44160196 | — |
| Product | HCID 45257317 | HCID 45257317 | — |
Reaction Steps
A solution of the compound of step 2 (23 mg, 43.4 μmol) in DCM (8 ml) and TFA (2 ml) was stirred at room temperature for 1 h. The solvents were evaporated and the resulting solid dissolved in MOH and water and lyophilized overnight. The title compound was obtained in the form of the [2-(5-fluoro-2-methyl-phenoxy)-1-phenyl-1H-indol-3-yl]-piperazin-1-yl-methanone trifluoroacetic acid salt as a white solid. Yield: 21.0 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211885B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-a39f97a2652b45ce9fe933b09208ee8e |
| Source note | uspto-grants-2012_07 |