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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1510062Generated: November 4, 2026

Trifluoroacetic acid → HCID 44160196, compound

https://huagongshe.com/reaction/1510062

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 66920434HCID 66920434—
SolventDichloromethaneHCID 6344—
ProductHCID 44160196HCID 44160196—
ProductHCID 45257317HCID 45257317—

Reaction Steps

A solution of the compound of step 2 (23 mg, 43.4 μmol) in DCM (8 ml) and TFA (2 ml) was stirred at room temperature for 1 h. The solvents were evaporated and the resulting solid dissolved in MOH and water and lyophilized overnight. The title compound was obtained in the form of the [2-(5-fluoro-2-methyl-phenoxy)-1-phenyl-1H-indol-3-yl]-piperazin-1-yl-methanone trifluoroacetic acid salt as a white solid. Yield: 21.0 mg.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08211885B2
Source datasetuspto-grants-2012_07
ORD IDord-a39f97a2652b45ce9fe933b09208ee8e
Source noteuspto-grants-2012_07