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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1510212Generated: November 4, 2026

Hydrogen Peroxide → HCID 69237532, compound

https://huagongshe.com/reaction/1510212

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen PeroxideHCID 784—
ReactantSodium HydroxideHCID 14798—
ReactantSodium borohydrideHCID 4311764—
ReactantHCID 69228053HCID 69228053—
SolventEthanolHCID 702—
SolventWaterHCID 962—
SolventTetrahydrofuranHCID 8028—
ProductHCID 69237532HCID 69237532—

Reaction Steps

With reference to FIG. 8, general procedure II was used. The quantities of the chemicals in order of addition are as follows: NaBH4 (0.029 g, 0.762 mmol), THF (10 ml), BF3-ether complex (0.1 ml, 0.81 mmol), (R)-2-(4-(2-(benzhydryloxy)ethyl)-5,6-dihydropyridin-1(2H)-yl)-1-(4-fluorophenyl)ethyl acetate 7c (0.180 g, 0.38 mmol), water (0.3 ml), ethanol (0.4 ml), 3N NaOH (0.3 ml) and 30% H2O2 (0.2 ml, 1.9 mmol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08211916B2
Source datasetuspto-grants-2012_07
ORD IDord-9e415b8d8fc24f4d91f943804c6e907b
Source noteuspto-grants-2012_07