HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69081370, compound → HCID 21226128, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69081370 | HCID 69081370 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21226128 | HCID 21226128 | 96.3% |
Reaction Steps
Benzyl ethyl 2,2′-(phenylimino)diacetate (1.0 g) was dissolved in methanol (15 mL) and 10% palladium on carbon (100 mg) was added to the mixture. The mixture was stirred at ambient temperature for 3 hours under hydrogen atmosphere (3 atms) and filtered through bed of celite. The filtrate was concentrated in vacuo to afford [(2-ethoxy-2-oxoethyl)(phenyl)amino]acetic acid (0.698 g) as a brown oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211919B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-625790e864644c5aa6cf531738709d0e |
| Source note | uspto-grants-2012_07 |