HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Isothiocyanato-3-(trifluoromethyl)benzene → HCID 86647224, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Isothiocyanato-3-(trifluoromethyl)benzene | HCID 137232 | — |
| Reactant | HCID 25002901 | HCID 25002901 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 86647224 | HCID 86647224 | 53.7% |
Reaction Steps
A solution of 1-(4,5-dihydrothiazol-2-yl)amino-1-(2,3-dichlorophenyl)-2-(3,5-dimethylphenyl)-ethane (0.25 g) in chloroform (10 ml) was treated with 1-isothiocyanato-3-trifluoromethylbenzene (0.13 g) at room temperature overnight. The solvent was evaporated in vacuo and the remainder was purified by column chromatography to yield 0.20 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211924B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-779a171b7f5e4b1da2c82630c09584fd |
| Source note | uspto-grants-2012_07 |