反应详情

In a reactor, 2 g of the compound obtained in Step B and 1 g of 5% palladium-on-carbon are introduced into a methano/THF 1/2 mixture under hydrogen pressure and at ambient temperature. After reacting for 8 hours, the reaction mixture is filtered. After evaporating off the solvents, the title product is obtained quantitatively with a chemical purity of 95%.

1. customat ambient temperature
2. filtrationthe reaction mixture is filtered
3. customAfter evaporating off the solvents