反应详情

To a solution of (29) (0.2 mmol, 36.8 mg) in 2 ml dichloroethane was added 0.2 mmol acetaldehyde, followed by 63.6 mg sodium triacetoxyborohydride, and 12 μl acetic acid. After 2 h, the solution was poured into water and extracted with ethyl acetate. The combined extracts were washed with water, dried over sodium sulfate, and the solvent removed by rotary evaporation.

1. extractionextracted with ethyl acetate
2. washThe combined extracts were washed with water
3. dry with materialdried over sodium sulfate
4. customthe solvent removed by rotary evaporation