化工社化工社 化学情報印刷レポート · 研究参考用
Benzene, 1,2-dichloro-3-fluoro- → 8-(2,3-Dichlorophenyloxy)-5-methyl-5,6,7,8-tetrahydro-4H-furo[3,2-c]azepine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzene, 1,2-dichloro-3-fluoro- | HCID 119011 | — |
| 反応物 | 5-methyl-5,6,7,8-tetrahydro-4H-furo[3,2-c]azepin-8-ol | HCID 68409910 | — |
| 生成物 | 8-(2,3-Dichlorophenyloxy)-5-methyl-5,6,7,8-tetrahydro-4H-furo[3,2-c]azepine | HCID 25027799 | — |
反応手順
The same method as in Example 1 was conducted using 5-methyl-5,6,7,8-tetrahydro-4H-furo[3,2-c]azepin-8-ol (Reference Example 21) instead of 6-methyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridin-4-ol (Reference Example 6) and was conducted using 2,3-dichloro-1-fluorobenzene instead of 1-fluoronaphthalene to give the objective compound.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US08217031B2 |
| 出典データセット | uspto-grants-2012_07 |
| ORD ID | ord-3178b58cb8fc4e2297f6e85dfa476c43 |
| 出典メモ | uspto-grants-2012_07 |