HRID1511714
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The free body of 8-(3,4-dichlorophenyloxy)-5-methyl-5,6,7,8-tetrahydro-4H-furo[3,2-c]azepine provided with Example 158 was dissolved in methanol, and then into the resulting methanol solution was added 1 equivalent of citric acid and was stirred for 1 hour. The mixture was concentrated to give the objective compound.
WORKUP
后处理
- concentrationThe mixture was concentrated
- customto give the objective compound