huagongshe.com
HRID1511798

反应详情

EQUATION

反应方程式

HRID 1511798 的结构方程式

REACTANTS

反应物

3
结构：CCCCCO
HCID6276

1-Pentanol

C5H12O

结构：CC(C)(C)OC(=O)NC1CCCNC1
HCID4233041

3-Boc-aminopiperidine

C10H20N2O2

结构：COc1ccc2nccc(Br)c2n1
HCID53421617

8-Bromo-2-methoxy-1,5-naphthyridine

C9H7BrN2O

PRODUCTS

生成物

1
结构：COc1ccc2nccc(N3CCCC(NC(=O)OC(C)(C)C)C3)c2n1
HCID66954590

未命名化合物

PROCEDURE

实验过程

According to procedure F and starting from 8-bromo-2-methoxy-[1,5]naphthyridine and (RS)-piperidin-3-yl-carbamic acid tert-butyl ester (commercial) and using 1-pentanol instead of NMP as reaction solvent, the title compound was isolated as an orange oil (2.44 g, 68%).

WORKUP

后处理

  1. customas reaction solvent