huagongshe.com
HRID1511951

反应详情

EQUATION

反应方程式

HRID 1511951 的结构方程式

REACTANTS

反应物

3
结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：Fc1cccc(F)c1CCl
HCID581570

2,6-Difluorobenzyl chloride

C7H5ClF2

结构：CC(C)(C)OC(=O)Nn1cccc1
HCID49760548

tert-Butyl 1H-pyrrol-1-ylcarbamate

C9H14N2O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N(Cc1c(F)cccc1F)n1cccc1
HCID67230234

未命名化合物

PROCEDURE

实验过程

Prepared according to the benzylation condition used in Example 1 step b) from pyrrol-1-yl-carbamic acid tert-butyl ester (1.0 eq.), 2,6-difluorobenzyl chloride (1.0 eq.) and sodium hydride (1.3 eq.). ESI (m/z): 309 (M+H)+.

WORKUP

后处理

  1. customPrepared