HRID1512566

反应详情

EQUATION

反应方程式

HRID 1512566 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

3

PROCEDURE

实验过程

1-{4′-[3-Methyl-4-(4-phenyl-but-1-enyl)-isoxazol-5-yl]-biphenyl-4-yl}-cyclopropanecarboxylic acid (0.030 g, 0.07 mmol) was dissolved in EtOAc and MeOH. 10% Palladium on carbon (spatula tip) was added, and the reaction was stirred under a balloon of H2 overnight. The mixture was filtered and concentrated to give the title compound.

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. concentrationconcentrated