HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 44549262, compound → HCID 53404692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 44549262 | HCID 44549262 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53404692 | HCID 53404692 | 98.9% |
Reaction Steps
A mixture of ethyl 4-methyl-5-nitropyridine-2-carboxylate (3.23 g) and 10% palladium-carbon powder (0.65 g) in ethanol (50 mL) was stirred at room temperature under a hydrogen atmosphere overnight. The insoluble material was removed by filtration, and the filtrate was concentrated under reduced pressure to give the title compound (2.74 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08217069B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-affccc2327f74309bef80e98dd2f71e6 |
| Source note | uspto-grants-2012_07 |