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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1512980Generated: November 3, 2026

HCID 44549262, compound → HCID 53404692, compound

https://huagongshe.com/reaction/1512980

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 44549262HCID 44549262—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 53404692HCID 5340469298.9%

Reaction Steps

A mixture of ethyl 4-methyl-5-nitropyridine-2-carboxylate (3.23 g) and 10% palladium-carbon powder (0.65 g) in ethanol (50 mL) was stirred at room temperature under a hydrogen atmosphere overnight. The insoluble material was removed by filtration, and the filtrate was concentrated under reduced pressure to give the title compound (2.74 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08217069B2
Source datasetuspto-grants-2012_07
ORD IDord-affccc2327f74309bef80e98dd2f71e6
Source noteuspto-grants-2012_07