HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 59496098, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | 6-phenyl-1,2,4-triazine-3,5(2h,4h)-dione | HCID 253363 | — |
| Product | HCID 59496098 | HCID 59496098 | 64.3% |
Reaction Steps
6-phenyl-1,2,4-triazine-3,5(2H,4H)-dione (prepared as described in BMCL, 2005, 43, 4363, 56 mg, 0.296 mmol) was heated in acetic anhydride (2 ml, 21.20 mmol) at 110° C. for 2 h, than was left at r.t. overnight. Solvent was evaporated under reduced pressure, obtaining 44 mg of title compound (64.3% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08217168B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-13c36f8a9fbf47089780f53016a0f194 |
| Source note | uspto-grants-2012_07 |