HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68433547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 25222719 | HCID 25222719 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 68433547 | HCID 68433547 | — |
Reaction Steps
6-methyl-2-(3-{(1S,5R)-1-[4-(trifluoromethyl)phenyl]-3-azabicyclo[3.1.0]hex-3-yl}propyl)-1,2,4-triazine-3,5(2H,4H)-dione was dissolved in Et2O and treated with HCl 1N in Et2O to form the title compound 6-methyl-2-(3-{(1S,5R)-1-[4-(trifluoromethyl)phenyl]-3-azabicyclo[3.1.0]hex-3-yl}propyl)-1,2,4-triazine-3,5(2H,4H)-dione hydrochloride salt (E2, 73.8 mg, 0.171 mmol).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08217168B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-ba943f30762c412086ce25e3523a34dd |
| Source note | uspto-grants-2012_07 |