Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 86653159 | HCID 86653159 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 74949036 | HCID 74949036 | — |
Reaction Steps
In an atmosphere of nitrogen, the 2,6,8-decatrienic acid toluene solution obtained in the above and DMF (3.7 g, 0.05 mol) were added to a 100 ml capacity flask, followed by cooling to 5° C. Thionyl chloride (11.9 g, 0.10 mol) was added dropwise to this and stirring was carried out at 5° C. for 0.5 hour to obtain a toluene solution of 2,6,8-decatrienoic acid chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08217192B2 |
|---|
| Source dataset | uspto-grants-2012_07 |
|---|
| ORD ID | ord-f8baae808ba9401d91ae0cd6a04dd613 |
|---|
| Source note | uspto-grants-2012_07 |
|---|
