反应详情

温度

5 °C

In an atmosphere of nitrogen, the 2,6,8-decatrienic acid toluene solution obtained in the above and DMF (3.7 g, 0.05 mol) were added to a 100 ml capacity flask, followed by cooling to 5° C. Thionyl chloride (11.9 g, 0.10 mol) was added dropwise to this and stirring was carried out at 5° C. for 0.5 hour to obtain a toluene solution of 2,6,8-decatrienoic acid chloride.

1. additionwere added to a 100 ml capacity flask