Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethylene Glycol → 2-hydroxyethoxy-acetic acid N,N-dimethylamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethylene Glycol | HCID 174 | — |
| 반응물 | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-hydroxyethoxy-acetic acid N,N-dimethylamide | HCID 16752596 | 35.5% |
반응 단계
The process according to Example 6 is followed with the difference that instead of ethylene glycol, toluene is used as solvent and 1 g tetrabutyl ammonium hydroxide is added to the reaction mixture. The yield is 5.22 g (35.5%) of the title compound having the purity higher than 98% as determined by gas chromatography.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08217200B2 |
| 출처 데이터셋 | uspto-grants-2012_07 |
| ORD ID | ord-5088c9b86fe94ffbab87776fba1f0507 |
| 출처 메모 | uspto-grants-2012_07 |