HRID1513553
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The process according to Example 6 is followed with the difference that instead of ethylene glycol, toluene is used as solvent and 1 g tetrabutyl ammonium hydroxide is added to the reaction mixture. The yield is 5.22 g (35.5%) of the title compound having the purity higher than 98% as determined by gas chromatography.