HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-3-butyn-2-ol → HCID 86637638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-3-butyn-2-ol | HCID 8258 | — |
| Reactant | Trimethylsilylacetylene | HCID 66111 | — |
| Reactant | HCID 59137864 | HCID 59137864 | — |
| Reactant | 9,9-Bis(3-methyl-4-aminophenyl)-2,7-bis(2-hydroxy-2-methyl-3-butynyl)fluorene | HCID 86637639 | — |
| Product | HCID 86637638 | HCID 86637638 | — |
Reaction Steps
Diethynylfluorene was synthesized by the same method as in the synthesis method of 9,9-bis(3-methyl-4-aminophenyl)-2,7-bis(trimethylsilylethynyl)fluorene represented by Example 1 except that trimethylsilylacetylene was replaced with 2-methyl-3-butyne-2-ol. The obtained compound was measured by the NMR and then the compound was 9,9-bis(3-methyl-4-aminophenyl)-2,7-bis(2-hydroxy-2-methyl-3-butynyl)fluorene represented by the following formula (3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08218937B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-34c20265ff674e9e9b2e7766057bf989 |
| Source note | uspto-grants-2012_07 |