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HRID1514045

反应详情

EQUATION

反应方程式

HRID 1514045 的结构方程式

REACTANTS

反应物

2
结构：O=C(Cl)Oc1cccc(C(F)(F)F)c1
HCID5057425

3-(Trifluoromethyl)phenyl chloroformate

C8H4ClF3O2

结构：C#CCC1CCN(C(=O)OC(C)(C)C)CC1
HCID18187546

未命名化合物

PRODUCTS

生成物

1
结构：C#CCC1CCN(C(=O)Oc2cccc(C(F)(F)F)c2)CC1
HCID57838900

未命名化合物

PROCEDURE

实验过程

3-(trifluoromethyl)phenyl chloroformate (5.0 g, 29.3 mmol) was added to a solution of tert-butyl 4-(prop-2-ynyl)piperidine-1-carboxylate (1.50 g, 6.72 mmol) according to general procedure 1. Yield=1.1031 g, 64%. m/z MH+=302.02. HPLC rt=10.8 min.

WORKUP

后处理

  1. customHPLC rt=10.8 min.