Cyclohexylamine → HCID 24825863, compound
Reaction equation
Cl[C:2]1[N:7]=[C:6](Cl)[CH:5]=[CH:4][N:3]=1.[CH:9]1([NH2:15])[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1.[NH:16]1[C:24]2[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH:18]=[N:17]1>>[CH:9]1([NH:15][C:6]2[CH:5]=[CH:4][N:3]=[C:2]([N:16]3[C:24]4[C:19](=[CH:20][CH:21]=[CH:22][CH:23]=4)[CH:18]=[N:17]3)[N:7]=2)[CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1Participants
4
Procedure
Was prepared according to Method A from 2,4-dichloropyrimidine, cyclohexylamine and indazole. LC-ESI-HRMS of [M+H]+ shows 294.173 Da. Calc. 294.17187 Da, dev. 3.8 ppm.
Workup
- customWas prepared
Sources & evidence
- ORD record
- ord-1e6263b176784be9bfc4121ccc4eaea4
- Source dataset
- uspto-grants-2012_07
- Patent number
- US08222262B2
Reaction notes
Loading…