4-Chloroaniline → HCID 24825963, compound

HRID 1514354Notes

Reaction equation

HRID 1514354 reaction equation
Cl[C:2]1[N:7]=[C:6](Cl)[CH:5]=[CH:4][N:3]=1.[Cl:9][C:10]1[CH:16]=[CH:15][C:13]([NH2:14])=[CH:12][CH:11]=1.[N+:17]([C:20]1[CH:21]=[C:22]2[C:26](=[CH:27][CH:28]=1)[NH:25][N:24]=[CH:23]2)([O-:19])=[O:18]>>[Cl:9][C:10]1[CH:16]=[CH:15][C:13]([NH:14][C:6]2[CH:5]=[CH:4][N:3]=[C:2]([N:24]3[CH:23]=[C:22]4[C:26]([CH:27]=[CH:28][C:20]([N+:17]([O-:19])=[O:18])=[CH:21]4)=[N:25]3)[N:7]=2)=[CH:12][CH:11]=1

Participants

4

Reactant 3

HCID 78124-ChloroanilineHCID 215015-NitroindazoleHCID 775312,4-Dichloropyrimidine

Product 1

HCID 24825963HCID 24825963, compound

Procedure

Was prepared according to Method A from 2,4-dichloropyrimidine, 4-chloroaniline and 5-nitroindazole. LC-ESI-HRMS of [M+H]+ shows 367.0692 Da. Calc. 367.071027 Da, dev. −5 ppm.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-44e9585ea6b0479d93a1b20527ac5a97
Source dataset
uspto-grants-2012_07
Patent number
US08222262B2

Reaction notes

Loading…