HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86638179, compound → HCID 86638180, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86638179 | HCID 86638179 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86638180 | HCID 86638180 | — |
Reaction Steps
A solution of 3-(4-formyl-3,5-dimethylphenyl)-acrylic acid tert-butyl ester (210 mg) in CH2Cl2 (8 mL) was hydrogenated at 1 atm over 10% Pd/C (21 mg) for 4 h. The catalyst was filtered and the filtrate concentrated to give 3-(4-formyl-3,5-dimethylphenyl)-propionic acid tert-butyl ester as a yellow solid. MS (ESI)m/z 286 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08222248B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-60b16fee257642adbde92ade0e8a4e1e |
| Source note | uspto-grants-2012_07 |