HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66965236, compound → HCID 66966238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66965236 | HCID 66965236 | — |
| Catalyst | Platinum oxide (PtO) | HCID 82844 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66966238 | HCID 66966238 | — |
Reaction Steps
A suspension of give 4-amino-N-isoquinolin-1-yl-3-nitrobenzamide and platinum oxide (330 mg) in MeOH (100 mL) was hydrogenated at 40 psi for 18 h. The catalyst was filtered from the solution through Celite and the filtrate evaporated to give 3,4-diamino-N-isoquinolin-1-yl-benzamide as a thick oil. MS (ESI) m/z 279.1 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08222248B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-bfbc9bf6628a4264845f6132dc0de96d |
| Source note | uspto-grants-2012_07 |