HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-diamino-N-(6-trifluoromethylpyridin-3-yl)-benzamide → HCID 178424983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-diamino-N-(6-trifluoromethylpyridin-3-yl)-benzamide | HCID 66965681 | — |
| Reactant | Methyl 3-(4-formyl-3,5-dimethylphenyl)-2,2-dimethylpropanoate | HCID 86632822 | — |
| Product | HCID 178424983 | HCID 178424983 | — |
Reaction Steps
The title compound was prepared from 3,4-diamino-N-(6-trifluoromethylpyridin-3-yl)-benzamide (from Example 6-36) and 3-(4-formyl-3,5-dimethylphenyl)-2,2-dimethylpropionic acid methyl ester analogous to Example 6-29. 1N NMR (400 MHz, MeOD): δ 9.20 (s, 1H), 8.68 (d, 1H), 8.43 (s, 1H), 8.10 (d, 1H), 7.98 (d, 1H), 7.85 (d, 1H), 7.19 (s, 2H), 3.00 (s, 2H), 2.27 (s, 6H), 1.29 (s, 6H). MS (m/z) 511.2 (M+1); Retention time: 1.20 min (Method 10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08222248B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-8c498e45672e436b92c00594e65af5a4 |
| Source note | uspto-grants-2012_07 |