HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-diamino-N-(6-trifluoromethylpyridin-3-yl)-benzamide → HCID 66966087, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-diamino-N-(6-trifluoromethylpyridin-3-yl)-benzamide | HCID 66965681 | — |
| Reactant | [(E)-3-(4-formyl-3,5-dimethylphenyl)-allyl]-phosphonic acid diethyl ester | HCID 86632823 | — |
| Product | HCID 66966087 | HCID 66966087 | — |
Reaction Steps
The title compound was prepared from 3,4-diamino-N-(6-trifluoromethylpyridin-3-yl)-benzamide and [(E)-3-(4-formyl-3,5-dimethylphenyl)-allyl]-phosphonic acid diethyl ester analogous to Example 6-32. 1H NMR (Methanol-d4, 400 MHz): δ 9.09 (d, 1H), 8.57 (dd, 1H), 8.34 (dd, 1H), 8.00 (dd, 1H), 7.87 (d, 1H), 7.76 (dd, 1H), 7.09 (s, 2H), 2.76 (t, 2H), 2.16 (s, 6H), 2.00 (m, 2H), 1.71 (m, 2H). MS (m/z) 533.1 (M+1); Retention time: 1.13 min (Method 10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08222248B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-6849a0dd1d54483fa3a9f8c502d95c16 |
| Source note | uspto-grants-2012_07 |