HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66966212, compound → HCID 86638181, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66966212 | HCID 66966212 | — |
| Catalyst | Manganese dioxide | HCID 14801 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86638181 | HCID 86638181 | — |
Reaction Steps
A mixture of [2-(2,6-dimethylphenyl)-3H-benzoimidazol-5-yl]-methanol (750 mg) and MnO2 (5 g) in THF (10 mL) was stirred at ambient temperature for 4 h. The mixture was filtered through Celite and the filtrate evaporated to give 2-(2,6-dimethyl-phenyl)-3H-benzoimidazole-5-carbaldehyde as an oil. MS (ESI)m/z 251 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08222248B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-ad8a804909874c08ba83963dff31c9d2 |
| Source note | uspto-grants-2012_07 |