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HRID1515564

反应详情

EQUATION

反应方程式

HRID 1515564 的结构方程式

REACTANTS

反应物

4
结构：COc1ccc(B(O)O)cc1OC
HCID2734702

3,4-Dimethoxyphenylboronic acid

C8H11BO4

结构：O.O=CC(=O)O
HCID15620607

Oxoacetic acid--water (1/1)

C2H4O4

结构：COc1ccc(C(Nc2cc(C)cc(C(N)=O)c2)C(=O)O)cc1OC
HCID59479497

2-(3-Carbamoyl-5-methylphenylamino)-2-(3,4-dimethoxyphenyl)acetic acid

C18H20N2O5

结构：COc1cc(N)cc(C(N)=O)c1
HCID59479527

3-Amino-5-methoxybenzamide

C8H10N2O2

PRODUCTS

生成物

1
结构：COc1cc(NC(C(=O)O)c2ccc(OC)c(OC)c2)cc(C(N)=O)c1
HCID59479457

未命名化合物

PROCEDURE

实验过程

Using a procedure analogous to that described for the preparation of 89D, 93D was reacted with 3,4-dimethoxyphenylboronic acid and glyoxylic acid monohydrate to give 93E. 1H NMR (400 MHz, CD3OD) δ ppm 3.73 (s, 3H) 3.80 (s, 3H) 3.81 (s, 3H) 5.07 (s, 1H) 6.39 (t, J=1.98 Hz, 1H) 6.75 (s, 1H) 6.81 (s, 1H) 6.92 (d, J=8.35 Hz, 1H) 7.07 (dd, J=8.35, 1.76 Hz, 1H) 7.11 (d, J=1.76 Hz, 1H).