Iodoethane → HCID 25266345, compound

HRID 1516401Notes

Reaction equation

HRID 1516401 reaction equation
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9]([C:11]2[CH:16]=[C:15]([Cl:17])[CH:14]=[CH:13][C:12]=2[NH:18][C:19]([C:21]2[CH:26]=[CH:25][C:24]([C:27]3[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=3[S:33]([CH3:44])(=[N:35][C:36]([CH:38]3[CH2:43][CH2:42][NH:41][CH2:40][CH2:39]3)=[O:37])=[O:34])=[CH:23][CH:22]=2)=[O:20])=[O:10])=[N:6][CH:7]=1.[CH2:45](I)[CH3:46]>>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([NH:8][C:9]([C:11]2[CH:16]=[C:15]([Cl:17])[CH:14]=[CH:13][C:12]=2[NH:18][C:19]([C:21]2[CH:22]=[CH:23][C:24]([C:27]3[CH:32]=[CH:31][CH:30]=[CH:29][C:28]=3[S:33]([CH3:44])(=[N:35][C:36]([CH:38]3[CH2:43][CH2:42][N:41]([CH2:45][CH3:46])[CH2:40][CH2:39]3)=[O:37])=[O:34])=[CH:25][CH:26]=2)=[O:20])=[O:10])=[N:6][CH:7]=1

Participants

3

Reactant 2

HCID 6340IodoethaneHCID 25266344HCID 25266344, compound

Product 1

HCID 25266345HCID 25266345, compoundYield 77%

Procedure

Product of Example 26 was ethylated using standard N-alkylating procedure with ethyl iodide to give titled compound in 77% yield.

Sources & evidence

ORD record
ord-62dcc6a5cd674d9ebb5a15c651d99111
Source dataset
uspto-grants-2012_07
Patent number
US08227492B2

Reaction notes

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