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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1516407Generated: November 4, 2026

Diethylamine → HCID 25270558, compound

https://huagongshe.com/reaction/1516407

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDiethylamineHCID 8021—
ReactantHCID 71540230HCID 71540230—
SolventWaterHCID 962—
SolventDimethylformamideHCID 6228—
ProductHCID 25270558HCID 2527055860%

Reaction Steps

To a stirring solution of S-[4-(N-{2-[N-(5-chloro(2-pyridyl))carbamoyl]-4-chlorophenyl}carbamoyl)phenyl]-S-methyl-N-[2-bromo-ethyl]sulfoximide (150 mg, 0.00026 mol) in DMF(0.7 mL) was added diethyl amine (1 mL) at 25° C. Reaction mixture was stirred at same temperature for 2 hr. Reaction mixture was diluted with water and filtered. Drying afforded 85 mg of titled compound in 60% yield.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08227492B2
Source datasetuspto-grants-2012_07
ORD IDord-c6932a2446654a0fb0dc365735d6df7b
Source noteuspto-grants-2012_07