HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodine chloride → HCID 490385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodine chloride | HCID 24640 | — |
| Reactant | HCID 490382 | HCID 490382 | — |
| Reactant | HCID 10331953 | HCID 10331953 | — |
| Solvent | Chloroform methanol | HCID 21584188 | — |
| Product | HCID 490385 | HCID 490385 | 29.6% |
Reaction Steps
Reaction of iodine monochloride (72.0 mg, 0.44 mmol) with 9a (95 mg, 0.39 mmol), using the procedure described for the preparation of 2c, and purification of the product by silica gel column chromatography using chloroform-methanol (90:10, v/v) as eluent afforded 10c as a syrup (48 mg, 29.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08227594B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-79dd2417fa3e447b8082a52ac75d3f09 |
| Source note | uspto-grants-2012_07 |