Didecyldimethylammonium → HCID 178443399, Verbindung

HRID 1517220Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1517220
[CH2:1]([N+:11]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])([CH3:13])[CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[Na+]>O>[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[CH2:14]([N+:11]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])([CH3:13])[CH3:12])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]

Komponenten

4

Edukt 2

HCID 16958DidecyldimethylammoniumHCID 16760658Sodium Salicylate

Produkt 1

HCID 178443399HCID 178443399, VerbindungAusbeute 90 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 962WaterLösungsmittel

Reaktionsbedingungen

Temperatur
60 °C

Versuchsvorschrift

The stechiometric amounts of didecyldimethylammonium saccharinate and sodium salicylate were mixed in distilled water and stirred at 60° C. for 2 h. After that time the solution was cooled to room temperature. The product was extracted from the aqueous solution with chloroform. The chloroform phase was removed and solvent was evaporated. Synthesized didecyldimethylammonium salicylate (90% yield) was dried under vacuum.

Aufarbeitung

  1. temperatureAfter that time the solution was cooled to room temperature
  2. extractionThe product was extracted from the aqueous solution with chloroform
  3. customThe chloroform phase was removed
  4. customsolvent was evaporated

Quellen und Nachweise

ORD-Eintrag
ord-0108f92853de4c5787c34919ef57250c
Quelldatensatz
uspto-grants-2012_07
Patentnummer
US08232265B2

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