HRID1517220

反应详情

EQUATION

反应方程式

HRID 1517220 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

CONDITIONS

反应条件

温度
60 °C

PROCEDURE

实验过程

The stechiometric amounts of didecyldimethylammonium saccharinate and sodium salicylate were mixed in distilled water and stirred at 60° C. for 2 h. After that time the solution was cooled to room temperature. The product was extracted from the aqueous solution with chloroform. The chloroform phase was removed and solvent was evaporated. Synthesized didecyldimethylammonium salicylate (90% yield) was dried under vacuum.

WORKUP

后处理

  1. temperatureAfter that time the solution was cooled to room temperature
  2. extractionThe product was extracted from the aqueous solution with chloroform
  3. customThe chloroform phase was removed
  4. customsolvent was evaporated