Didecyldimethylammonium → HCID 178443399、化合物

HRID 1517220ノート

反応式

HRID 1517220 の反応式
[CH2:1]([N+:11]([CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23])([CH3:13])[CH3:12])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10].[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[Na+]>O>[C:24]([O-:33])(=[O:32])[C:25]1[C:26](=[CH:28][CH:29]=[CH:30][CH:31]=1)[OH:27].[CH2:14]([N+:11]([CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH3:10])([CH3:13])[CH3:12])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH3:23]

参加物

4

反応物 2

HCID 16958DidecyldimethylammoniumHCID 16760658Sodium Salicylate

生成物 1

HCID 178443399HCID 178443399、化合物収率 90%

試薬・触媒・溶媒 1

HCID 962Water溶媒

反応条件

温度
60 °C

実験手順

The stechiometric amounts of didecyldimethylammonium saccharinate and sodium salicylate were mixed in distilled water and stirred at 60° C. for 2 h. After that time the solution was cooled to room temperature. The product was extracted from the aqueous solution with chloroform. The chloroform phase was removed and solvent was evaporated. Synthesized didecyldimethylammonium salicylate (90% yield) was dried under vacuum.

後処理

  1. temperatureAfter that time the solution was cooled to room temperature
  2. extractionThe product was extracted from the aqueous solution with chloroform
  3. customThe chloroform phase was removed
  4. customsolvent was evaporated

出典と根拠

ORDレコード
ord-0108f92853de4c5787c34919ef57250c
出典データセット
uspto-grants-2012_07
特許番号
US08232265B2

反応ノート

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