Didecyldimethylammonium Chloride → HCID 69295561, compound

HRID 1517224Notes

Reaction equation

HRID 1517224 reaction equation
[Cl-].[CH2:2]([N+:12]([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24])([CH3:14])[CH3:13])[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11].[Na+].[C:26]([O-:34])(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1>O>[C:26]([O-:34])(=[O:33])[C:27]1[CH:32]=[CH:31][CH:30]=[CH:29][CH:28]=1.[CH2:15]([N+:12]([CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])([CH3:14])[CH3:13])[CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

4

Reactant 2

HCID 23558Didecyldimethylammonium ChlorideHCID 517055Sodium Benzoate

Product 1

HCID 69295561HCID 69295561, compoundYield 85%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Conditions

Temperature
80 °C

Procedure

Didecyldimethylammonium chloride (0.02 mol) was dissolved in distilled water and 0.015 mol of benzoic acid sodium salt was added. The solution was stirred at 80° C. for 7 h. The reaction mixture was extracted by chloroform. Chloroform phase was removed and washed with distilled, cold water until chloride ions were no longer detected using AgNO3. Then chloroform was removed. Obtainede benzoate in 85% yield was dried in vacuum. 1H NMR and 13C NMR (CDCl3) were obtained.

Workup

  1. extractionThe reaction mixture was extracted by chloroform
  2. customChloroform phase was removed
  3. washwashed
  4. distillationwith distilled
  5. customThen chloroform was removed
  6. dry with materialObtainede benzoate in 85% yield was dried in vacuum
  7. custom1H NMR and 13C NMR (CDCl3) were obtained

Sources & evidence

ORD record
ord-93fae666c580449cb57d3b79dc306177
Source dataset
uspto-grants-2012_07
Patent number
US08232265B2

Reaction notes

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