Sodium Chloride → HCID 69295523, compound

HRID 1517225Notes

Reaction equation

HRID 1517225 reaction equation
[Cl-].[OH:2][CH2:3][CH2:4][N+:5]([CH2:8][O:9][CH:10]1[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1)([CH3:7])[CH3:6].[C:22]([O-:30])(=[O:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1.[Na+].[Na+].[Cl-]>CC(C)=O>[C:22]([O-:30])(=[O:29])[C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][CH:24]=1.[OH:2][CH2:3][CH2:4][N+:5]([CH2:8][O:9][CH:10]1[CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11]1)([CH3:7])[CH3:6]

Participants

5

Reactant 3

HCID 5234Sodium ChlorideHCID 517055Sodium BenzoateHCID 69294846HCID 69294846, compound

Product 1

HCID 69295523HCID 69295523, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

0.1 mol of (2-hydroxyethyl)cyclododecyloxymethyldimethylammonium chloride was dissolved in 100 mL of anhydrous acetone and sodium benzoate was added. After 5 h of stirring, NaCl was filterd and the reaction mixture was concentrated using a rotary evaporator. The obtained was dried for 10 h at 50° C. in vacuum.

Workup

  1. concentrationthe reaction mixture was concentrated
  2. customa rotary evaporator
  3. customThe obtained was dried for 10 h at 50° C. in vacuum

Sources & evidence

ORD record
ord-c1f741c692d24cd092280c24a1bf714b
Source dataset
uspto-grants-2012_07
Patent number
US08232265B2

Reaction notes

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